火焰原子吸收光谱法测定钴-镍合金镀层中的钴和镍

利用原子吸收光谱法研究了在氨基磺酸钴-镍镀液中，赫尔槽试片上不同电流密度区合金镀层中钴、镍的含量。实验表明，该方法简便，快捷，结果准确，精密度高。相对标准偏差（RSD）为0.30%-0.62%，加标回收率为97.0%-104.0%。     

双线性系统的无反馈解耦线性化

用现代微分几何方法研究了双线性控制系统的解耦线性化问题，给出了一般双线性系统解耦线性化的充分条件及严格双线性系统解耦线性化的充要条件，并举例说明了本文的结论。     

Validation of fuzzy logic method for automated mass spectral classification for mineral imaging

Imaging mass spectrometry requires the acquisition and interpretation of hundreds to thousands of individual spectra in order to map the mineral phases within heterogeneous geomatrices. A fuzzy logic inference engine (FLIE) was developed to automate data interpretation. To evaluate the strengths and limitations of FLIE, the chemical images obtained using FLIE were compared with those developed using two chemometric methods: principle component analysis (PCA) and cluster analysis (K-Means). Two heterogeneous geomatrices, a low-grade chalcopyrite ore and basalt, were imaged using a laser-desorption Fourier transform mass spectrometer. Similar mineral distribution patterns in the chalcopyrite ore sample were obtained by the three data analysis methods with most of the differences occurring at the interfaces between mineral phases. PCA missed one minor mineral phase in the chalcopyrite ore sample and did not clearly differentiate among the mineral classes of the basalt. K-Means cluster analysis differentiated among the various mineral phases in both samples, but improperly grouped some spectra in the chalcopyrite sample that only contained unanticipated high mass peaks. Unlike the chemometric methods, FLIE was able to classify spectra as unknowns for those spectra that fell below the confidence level threshold. A nearest neighbor approach, included in FLIE, was used to classify the unknowns to form a visually complete image; however, the unknowns identified by FLIE can be informative because they highlight potential problems or overlooked results. In conclusion, this study validated the fuzzy logic-based approach used in our laboratory and reveald some limitations in the three techniques that were evaluated.     

屋顶绿化的自动灌溉系统设计

屋顶绿化对提高城市空气质量、减少“热岛效应”、改善居住环境有积极的意义，但其灌溉环节与普通园林绿化灌溉相比有更高的要求．为了增强屋顶灌溉的科学性，根据其特点提出了建立自动灌溉系统的设想，并对灌溉过程建立了混杂自动机模型，从离散事件动态系统与连续变量动态系统的角度共同描述了自动灌溉的过程，最后给出了自动灌溉系统的工程设计方案，对屋顶绿化自动化、精细化程度的提高具有一定的启示意义．     

四（对-羟基苯基）卟啉氧合配合物的室温固相合成，表征及氧合能力

采用固相反应合成了四羟基苯基卟啉与与Fe^2＋,Co^2＋金属离子的配合物,在室温下,将其与分子O2作用,提纯后得到两种固态氧合配合物．通过元素分析、红外光谱（IR）、核磁共振氢谱（^1HNMR）、电导、热分析（TG／DTA）、紫外光谱（UV）等测试手段确定了氧合配合物的组成为[Co·THPP·O2]（NO3）2·2H2O、[Fe·THPP·O2]Cl2·2H2O]，可知1mol配合物吸收了1molO2,采用失重法测定了氧合配合物中的配位氧,确定1mol金属配合物吸收1molO2形成超氧配合物．     

关于SIS环

通过自内射环和半本原环给出了SIS环的定义,即如果RRR是内射的并且J(R)=0,我们称此环为SIS环;并且得到了它的一些刻画和性质.     

中物院远红外自由电子激光实验研究

中国工程物理研究院基于射频直线加速器技术的远红外自由电子激光(FIR-FEL)实验取得阶段性进展,于2005年3月24晚8时30分首次出光, 并多次重复. 中心波长115μm, 谱宽1%.介绍了实验系统的主要组成部分和主要实验结果.     

航空兵塔台辅助指挥系统通信分系统技术设计方案

文章详细描述了航空兵机场塔台辅助指挥系统之通信分系统设计的特点与功能、硬件结构、软件设计原则以及接口通信协议等问题。该分系统设计已在航空兵塔台辅助指挥系统研究中得到应用 ,并达到了良好的控制效果。